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Key Information :

  • Measurement stations : 3 adsorption station (non-corrosive gas probe molecules). No degassing independent system but second degassing phase on the analysis ports at room temperature
    • Pressure range : Meso- and macro-porosity : 1 to 760 mmHg (10 to 10⁵ Pa)
    • Pressure sensors : 1000 mmHg (resolution 10⁻³ mmHg) for the 3 ports
  • Analysis temperature : 77K (liquid nitrogen), 273K (ice bath), 293 K (room temperature). The analysis temperature is common for the 3 analysis port
  • Adsorbates : non-corrosive gas –  no vapor
  • Specific surface area : > 0. 1 m²/g (N₂)
  • Degassing station : No degassing stations. Second degassing on the analysis ports : at room temperature to 350 °C (increment of 0,1°C)
  • Cryogenic system : 3.5-liter Dewar, 48 h autonomy
  • Accessibility : Self-service for staff, PhD students, and Master’s students after training by the technical manager

 

Specific Surface Area and Porosity Analyzer – Micromeritics Tristar

The Tristar is a device dedicated to measuring the textural properties (specific surface area, porosity) of the MESOPOROUS materials It allows for the characterization of meso- and macroporous structures. A preliminary external degassing (activation) phases must be done before adsorption analysis. A second degassing phase is possible on the analysis port a room temperature.

Typical Uses :

The Tristar is used for :

  • Characterizing the  meso- and macro-porosity of materials
  • Specific surface area,
  • Pore size distribution, geometry (BJH et DFT models)

Preliminary treatment : removing impurities through degassing prior to analysis

Fields of Application

  • Porous inorganic or carbonaceous (mesoporous)
  • Polymer and polymer-based composite materials
  • Bio-based and nanostructured materials
  • Applications in advanced materials and the chemical industry

Available Measurements

  • Specific surface area
  • Porosity analysis : pore size distribution, pore volume, geometry